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Determination of sulfhydryl content in CTS?GSH through near-infrared reflectance spectroscopy

  • Peng ZHANG Yulu Wang Guocheng ZHU Zhaojie JIAO Wei ZHANG
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  • 1. School of Civil Engineering, Hunan University of Science and Technology, Xiangtan, Hunan 411201, China
    2. Engineering Research Center for Waste Oil Recovery Technology and Equipment of Ministry of Education,Chongqing Technology
    and Business University, Chongqing 400067, China

Received date: 2017-11-16

  Revised date: 2018-01-18

  Online published: 2018-08-15

Abstract

The thiolated chitosan (CTS?GSH) was synthesized via the amidation reaction of chitosan (CTS) with reduced glutathione (GSH). A total of 56 samples were scanned with near-infrared reflectance spectroscopy (NIRS) instrument. The characteristic absorption peaks of each band were selected as independent variables, and sulfhydryl content as the dependent variable, the partial least squares (PLS) model was established. Sulfhydryl content was predicted by the PLS, and predicted values were compared with measured values. The results showed that the correlation coefficient of the measured and predicated values of sulfhydryl content was more than 0.9, presenting a good forecasting performance of the model. The difference between the predicted and measured values was nonsignificant, suggesting the feasibility of predicting sulfhydryl content in CTS?GSH through NIRS.

Cite this article

Peng ZHANG Yulu Wang Guocheng ZHU Zhaojie JIAO Wei ZHANG . Determination of sulfhydryl content in CTS?GSH through near-infrared reflectance spectroscopy[J]. The Chinese Journal of Process Engineering, 2018 , 18(4) : 757 -763 . DOI: 10.12034/j.issn.1009-606X.217390

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