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Fe2+掺杂秸秆黑炭电极的制备及对水中Zn2+的吸附

  • 谢永 陈祥凤 赵国庆 王红艳 张瑞
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  • 宿州学院化学化工学院 宿州学院化学化工学院 宿州学院化学化工学院 四川大学原子与分子物理所 宿州学院化学化工学院

收稿日期: 2015-02-10

  修回日期: 2015-05-13

  网络出版日期: 2015-08-20

Preparation of Fe2+-doped Straw Carbon Electrode and Its Adsorption Properties to Zn2+ from Wastewater

  • XIE Yong CHEN Xiang-feng ZHAO Guo-qing WANG Hong-yan ZHANG Rui
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  • School of chemistry & chemical engineering, Suzhou University School of chemistry & chemical engineering, Suzhou University School of chemistry & chemical engineering, Suzhou University Institute of Atomic and Molecular Physics, Sichuan University School of chemistry & chemical engineering, Suzhou University

Received date: 2015-02-10

  Revised date: 2015-05-13

  Online published: 2015-08-20

摘要

:将玉米秸秆无氧炭化,以葡萄糖为粘合剂掺杂Fe2+水热制备秸秆炭电极,表征了其结构和形貌,考察了电压、时间、pH值对Fe2+炭化电极吸附模拟废水中Zn2+的影响. 结果表明,玉米秸秆与FeSO4×7H2O按质量比1:1所制电极疏松多孔、鼓泡均匀. 在电压14 V、pH值8.0、吸附150 min的条件下,对Zn2+的去除率达88.2%.

本文引用格式

谢永 陈祥凤 赵国庆 王红艳 张瑞 . Fe2+掺杂秸秆黑炭电极的制备及对水中Zn2+的吸附[J]. 过程工程学报, 2015 , 15(4) : 708 -712 . DOI: 10.12034/j.issn.1009-606X.215142

Abstract

Corn straw was carbonized in a non-oxygen atmosphere to obtain straw carbon, and Fe2+-doped carbon electrode was synthesized by hydrothermal method with glucose as adhesive through the reaction of FeSO4×7H2O with the straw carbon. Its microstructure and morphology were analyzed. The effects of voltage, time and pH value on adsorption removal of Zn2+ from wastewater by the Fe2+ doped carbon electrode were examined. The results show that the electrode has a best adsorption rate of 88.2% when the mass ratio of corn straw carbon to FeSO4×7H2O is 1:1 and under the conditions of adsorption at the voltage of 14 V, 150 min and pH 8.0.
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